Ultra-high resolution <sup>17</sup>O solid-state NMR spectroscopy of biomolecules: A comprehensive spectral analysis of monosodium L-glutamate·monohydrate

Symplectic ID:

164242

Source:

Scopus

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Monday, 14 September, 2026 - 00:34

DOI:

10.1039/c1cp20629j

Publication Date:

Thursday, 14 July, 2011

First Page:

12213

Last Page:

12224

Authors:

Wong, A

Howes, AP

Yates, JR

Watts, A

Anupõld, T

Past, J

Samoson, A

Dupree, R

Smith, ME

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0

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Abstract:

Monosodium L-glutamate monohydrate, a multiple oxygen site (eight) compound, is used to demonstrate that a combination of high-resolution solid-state NMR spectroscopic techniques opens up new possibilities for 17O as a nuclear probe of biomolecules. Eight oxygen sites have been resolved by double rotation (DOR) and multiple quantum (MQ) NMR experiments, despite the 17O chemical shifts lying within a narrow shift range of

ISSN:

1463-9076

Journal Title:

Physical Chemistry Chemical Physics

Volume:

13

Issue:

26

ID at Source:

2-s2.0-79959480355

Publication Status:

Published

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oums0549