Effects of polymer infiltration processing (PIP) temperature on the mechanical and thermal properties of Nextel 312 fibre SiCO ceramic matrix composites

Pirzada T, Singh S, Meyere R, Earp P, Galano M, Marrow T

© 2020 Elsevier Ltd Effects of the polymer infiltration processing (PIP) temperature between 850 and 1050 °C on the mechanical and thermal properties of Nextel 312 fibre SiCO ceramic matrix composite were studied. The aim was to optimise the material system for its proposed application as a mechanical gas-seal at temperatures up to 900 °C. The microstructure and its failure behaviour at room temperature were characterised using electron microscopy (SEM, TEM), X-ray diffraction and high resolution X-ray Tomography, with mechanical testing by nano-indentation, fibre-push out and flexural bending. Thermo-gravimetric analysis quantified the thermal stability. Processing at 950 °C or above gave a combination of high effective elastic modulus, good resistance to mechanical damage from tensile strain and good thermal stability.